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Front Cover Picture: Two‐Step Continuous‐Flow Synthesis of Fungicide Metalaxyl through Catalytic C−N Bond‐Formation Processes (Adv. Synth. Catal. 1/2022)
Front Cover Picture: Two‐Step Continuous‐Flow Synthesis of Fungicide Metalaxyl through Catalytic C−N Bond‐Formation Processes (Adv. Synth. Catal. 1/2022)
The front cover picture, depicts Metalaxyl, an acylalanine fungicide, which was synthesized through catalytic continuous s...
Tris(pentafluorophenyl)borane‐Catalyzed Oxygen Insertion Reaction of α‐Diazoesters (α‐Diazoamides) with Dimethyl Sulfoxide
Tris(pentafluorophenyl)borane‐Catalyzed Oxygen Insertion Reaction of α‐Diazoesters (α‐Diazoamides) with Dimethyl Sulfoxide
A tris(pentafluorophenyl)borane-catalyzed oxidation reaction of α-diazoesters (α-diazo amides) with dimethyl s...
A Synthetic Protocol for the Construction of Chroman‐Spiroquinazolin(thi)one Framework via a Metal‐Free, Three‐Component, Domino, Double Annulations
A Synthetic Protocol for the Construction of Chroman‐Spiroquinazolin(thi)one Framework via a Metal‐Free, Three‐Component, Domino, Double Annulations
A three-component domino approach for the synthesis of chroman-spiroquinazolin(thi)ones is described. It involves a conden...
Synthesis of SCF3‐Substituted Sulfonium Ylides from Sulfonium Salts or α‐Bromoacetic Esters
Synthesis of SCF3‐Substituted Sulfonium Ylides from Sulfonium Salts or α‐Bromoacetic Esters
A metal-free direct trifluoromethylthiolation of sulfonium ylides with an electrophilic trifluoromethylthiolating reagent ...
Electrochemical Ammonium Cation‐Assisted Hydropyridylation of Ketone‐Activated Alkenes: Experimental and Computational Mechanistic Studies
Electrochemical Ammonium Cation‐Assisted Hydropyridylation of Ketone‐Activated Alkenes: Experimental and Computational Mechanistic Studies
Abstract. This work describes an electrochemical ammonium cation enabled hydropyridylation of ketone-activated alkenes und...
Hydrogenation of Esters by Manganese Catalysts
Hydrogenation of Esters by Manganese Catalysts
The hydrogenation of esters catalyzed by a manganese complex of phosphine-aminopyridine ligand was developed. Using this p...
Synthesis of Enantioenriched Amines by Iron‐Catalysed Amination of Alcohols Employing at Least One Achiral Substrate
Synthesis of Enantioenriched Amines by Iron‐Catalysed Amination of Alcohols Employing at Least One Achiral Substrate
Abstract The synthesis of a broad range of enantioenriched amines by the direct Fe-catalysed coupling of amines with alcoh...
Front Cover Picture: Synthesis of Enantioenriched Amines by Iron‐Catalysed Amination of Alcohols Employing at Least One Achiral Substrate (Adv. Synth. Catal. 24/2021)
Front Cover Picture: Synthesis of Enantioenriched Amines by Iron‐Catalysed Amination of Alcohols Employing at Least One Achiral Substrate (Adv. Synth. Catal. 24/2021)
The Front Cover Picture, designed by Anastasiia Afanasenko, illustrates the methodology for the synthesis of enantioenrich...
Diastereoselective Bidirectional C(sp3)‐H Bond Functionalization of Piperazine Compounds
Diastereoselective Bidirectional C(sp3)‐H Bond Functionalization of Piperazine Compounds
A highly diastereoselective bidirectional C(sp3)-H bond functionalization of piperazine compounds, triggered by a Lewis ac...
Electrochemically Mediated Direct C(sp3)‐H Sulfonylation of Xanthene Derivatives
Electrochemically Mediated Direct C(sp3)‐H Sulfonylation of Xanthene Derivatives
The construction of C(sp3)-sulfonyl bonds through direct sulfonylation of C(sp3)-H bond presents a number of challenges, s...
Stereoselective Cyclopropanation of Boron Dipyrromethene (BODIPY) Derivatives by an Organocascade Reaction
Stereoselective Cyclopropanation of Boron Dipyrromethene (BODIPY) Derivatives by an Organocascade Reaction
Abstract The synthesis of enantiopure chiral boron dipyrromethenes (BODIPYs) is of importance due the intrinsic properties...
Rhodium(III)‐Catalyzed Aldehyde C‐H Activation and Functionalization with Dioxazolones: An Entry to Imide Synthesis
Rhodium(III)‐Catalyzed Aldehyde C‐H Activation and Functionalization with Dioxazolones: An Entry to Imide Synthesis
A rhodium(III)-based catalytic system has been used to develop a C-H bond activation of benzaldehyde derivatives and subse...
Ruthenium‐Catalyzed Vinylene Carbonate Annulation by C–H/N–H Functionalizations: Step‐Economical Access to Indoles
Ruthenium‐Catalyzed Vinylene Carbonate Annulation by C–H/N–H Functionalizations: Step‐Economical Access to Indoles
A convenient and effective method of ruthenium-catalyzed C–H/N–H annulations using vinylene carbonate as oxi...
Pd‐Catalyzed Atropselective C‐H Olefination Promoted by a Transient Directing Group
Pd‐Catalyzed Atropselective C‐H Olefination Promoted by a Transient Directing Group
A Pd(II)-catalyzed atroposelective olefination of biaryls with maleimides is reported using chiral transient directing gro...
Visible‐Light‐Assisted Synthesis of Allylic Triflamides via Dual Acridinium/Co Catalysis
Visible‐Light‐Assisted Synthesis of Allylic Triflamides via Dual Acridinium/Co Catalysis
An efficient dehydrogenative functionalization of styryl carbon-carbon double bonds with triflamide is described via dual ...
BiCl3‐Mediated Tandem Cyclization of Tryptamine‐Derived Ynamide: Concise Synthesis of Pentacyclic Spiroindolines and Tricyclic Indole Derivatives
BiCl3‐Mediated Tandem Cyclization of Tryptamine‐Derived Ynamide: Concise Synthesis of Pentacyclic Spiroindolines and Tricyclic Indole Derivatives
Catalytic tandem cyclization of ynamides has attracted considerable interest in organic synthesis because of its atom econ...
Palladium‐Catalyzed Carbamoyl‐Carbamoylation/ Carboxylation/Thioesterification of Alkene‐Tethered Carbamoyl Chlorides using Mo(CO)6 as the Carbonyl Source
Palladium‐Catalyzed Carbamoyl‐Carbamoylation/ Carboxylation/Thioesterification of Alkene‐Tethered Carbamoyl Chlorides using Mo(CO)6 as the Carbonyl Source
We reported a palladium-catalyzed carbamoyl-carbamoylation/carboxylation/thioesterification of alkene-tethered carbamoyl c...
Asymmetric Synthesis of Chiral α‐CF2H spiro[indoline‐3,3'‐thiophene] via Phase‐Transfer Catalyzed Sulfa‐Michael/Michael Domino Reaction
Asymmetric Synthesis of Chiral α‐CF2H spiro[indoline‐3,3'‐thiophene] via Phase‐Transfer Catalyzed Sulfa‐Michael/Michael Domino Reaction
Abstract. An efficient and practical sulfa-Michael/Michael domino reaction of (E)-4-mercapto-2-butenoates with difluoromet...
Minisci‐type Alkylation of N‐Heteroarenes by N‐(Acyloxy)phthalimides Mediated by a Hantzsch Ester and Blue LED Light
Minisci‐type Alkylation of N‐Heteroarenes by N‐(Acyloxy)phthalimides Mediated by a Hantzsch Ester and Blue LED Light
A synthetic method that enables the Hantzsch ester-mediated Minisci-type C2-alkylation of quinolines, isoquinolines and py...
H2O2‐Mediated Synthesis of 1,2,4‐Thiadiazole Derivatives in Ethanol at Room Temperature
H2O2‐Mediated Synthesis of 1,2,4‐Thiadiazole Derivatives in Ethanol at Room Temperature
Herein, we report the H2O2-mediated synthesis of 1,2,4-thiadiazole derivatives under metal-free conditions at room tempera...
Iron‐Catalyzed One‐step Synthesis of Isothiazolone/1,2‐Selenazolone Derivatives via [3+1+1] Annulation of Cyclopropenones, Anilines, and Elemental Chalcogens
Iron‐Catalyzed One‐step Synthesis of Isothiazolone/1,2‐Selenazolone Derivatives via [3+1+1] Annulation of Cyclopropenones, Anilines, and Elemental Chalcogens
Described herein is the one-step synthesis of isothiazolone/1,2-selenazolone derivatives via [3+1+1] cycloaddition of cycl...
Nickel‐Catalyzed Decarbonylative Cycloaddition of Benzofuran‐2,3‐diones with Alkynes to Flavones
Nickel‐Catalyzed Decarbonylative Cycloaddition of Benzofuran‐2,3‐diones with Alkynes to Flavones
Using dppe as the ligand, the Nickel-catalyzed decarbonylative cycloaddition of benzofuran-2,3-diones with alkynes was est...
Rhodium‐Catalysed Asymmetric Arylation of Pyridylimines
Rhodium‐Catalysed Asymmetric Arylation of Pyridylimines
The catalytic asymmetric arylation of pyridylimines was developed. A range of pyridylimines reacted with arylboronic acids...
Front Cover Picture: Lewis Acid‐Catalyzed Formal (4+2)‐ and (2+2+2)‐Cycloaddition Between 1‐Azadienes and Styrylmalonates as Analogues of Donor‐Acceptor Cyclopropanes (Adv. Synth. Catal. 23/2021)
Front Cover Picture: Lewis Acid‐Catalyzed Formal (4+2)‐ and (2+2+2)‐Cycloaddition Between 1‐Azadienes and Styrylmalonates as Analogues of Donor‐Acceptor Cyclopropanes (Adv. Synth. Catal. 23/2021)
The front cover picture, designed by Pavel G. Sergeev and Daria I. Filina, illustrates the comparison between reactivities...
Acridine Orange Hemi(Zinc Chloride) Salt as a Lewis Acid‐Photoredox Hybrid Catalyst for the Generation of α‐Carbonyl Radicals
Acridine Orange Hemi(Zinc Chloride) Salt as a Lewis Acid‐Photoredox Hybrid Catalyst for the Generation of α‐Carbonyl Radicals
Abstract A readily accessible organic-inorganic hybrid catalyst is reported for the reductive fragmentation of α-hal...
The regioselective Arylation of 1,3‐Benzodioxoles
The regioselective Arylation of 1,3‐Benzodioxoles
The direct arylation of 1,3-benzodioxole and 2,2-difluorobenzo[1,3]dioxole with 28 different aryl bromides yields the resp...
Combined Photoredox and Carbene Catalysis for the Synthesis of γ‐Aryloxy Ketones
Combined Photoredox and Carbene Catalysis for the Synthesis of γ‐Aryloxy Ketones
N-heterocyclic carbenes (NHCs) have emerged as catalysts for the construction of C–C bonds in the synthesis of subs...
Calcium‐Catalyzed Intramolecular Hydroamination‐Deacylation Reaction of in situ formed β‐Amino Allenes
Calcium‐Catalyzed Intramolecular Hydroamination‐Deacylation Reaction of in situ formed β‐Amino Allenes
We have developed a simple, One-Pot, three-component reaction of tert-propargyl alcohols, primary amines and acyl ketones ...
Synthesis of Substituted 1‐Hydroxy‐2‐naphthaldehydes by Rhodium‐Catalyzed C‒H Bond Activation and Vinylene Transfer of Enaminones with Vinylene Carbonate
Synthesis of Substituted 1‐Hydroxy‐2‐naphthaldehydes by Rhodium‐Catalyzed C‒H Bond Activation and Vinylene Transfer of Enaminones with Vinylene Carbonate
The rhodium(III)-catalyzed C‒H bond activation and vinylene transfer of enaminones with vinylene carbonate have bee...
Gold(I)‐Catalyzed Selective Cyclization and 1,2‐Shift to Prepare Pseudorutaecarpine Derivatives
Gold(I)‐Catalyzed Selective Cyclization and 1,2‐Shift to Prepare Pseudorutaecarpine Derivatives
A variety of pseudorutaecarpine derivatives were prepared in good to excellent yields through a gold(I)-catalyzed selectiv...
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