Sargent, M. (Ed. ). Guide to achieving reliable quantitative LC-MS measurements; LGC, 2013.
Yan Z, Maher N, Torres R, Cotto C, Hastings B, Dasgupta M, Hyman R, Huebert N, Caldwell GW. Isobaric metabolite interferences and the requirement for close examination of raw data in addition to stringent chromatographic separations in liquid chromatography/tandem mass spectrometric analysis of drugs in biological matrix. Rapid Commun. Mass Spectrom. 2008;22(13):2021–8. https://doi.org/10.1002/rcm.3577.
Article CAS PubMed Google Scholar
Uclés S, Lozano A, Sosa A, Parrilla Vázquez P, Valverde A, Fernández-Alba AR. Matrix interference evaluation employing GC and LC coupled to triple quadrupole tandem mass spectrometry. Talanta. 2017;174:72–81. https://doi.org/10.1016/j.talanta.2017.05.068.
Article CAS PubMed Google Scholar
Memboeuf A, Jullien L, Lartia R, Brasme B, Gimbert Y. Tandem mass spectrometric analysis of a mixture of isobars using the survival yield technique. J. Am. Soc. Mass Spectrom. 2011;22(10) https://doi.org/10.1007/s13361-011-0195-8.
Josse T, Winter JD, Dubois P, Coulembier O, Gerbaux P, Memboeuf A. A tandem mass spectrometry-based method to assess the architectural purity of synthetic polymers: a case of a cyclic polylactide obtained by click chemistry. Polym. Chem. 2014;6(1):64–9. https://doi.org/10.1039/C4PY01087F.
Jeanne Dit Fouque D, Maroto A, Memboeuf A. Purification and quantification of an isomeric compound in a mixture by collisional excitation in multistage mass spectrometry experiments. Anal. Chem. 2016;88(22):10821–5. https://doi.org/10.1021/acs.analchem.6b03490.
Article CAS PubMed Google Scholar
Jeanne Dit Fouque D, Lartia R, Maroto A, Memboeuf A. Quantification of intramolecular click chemistry modified synthetic peptide isomers in mixtures using tandem mass spectrometry and the survival yield technique. Anal. Bioanal. Chem. 2018;410(23):5765–77. https://doi.org/10.1007/s00216-018-1258-5.
Article CAS PubMed Google Scholar
Jeanne Dit Fouque D, Maroto A, Memboeuf A. Internal standard quantification using tandem mass spectrometry of a tryptic peptide in the presence of an isobaric interference. Anal. Chem. 2018;90(24):14126–30. https://doi.org/10.1021/acs.analchem.8b05016.
Article CAS PubMed Google Scholar
Maroto A, Jeanne Dit Fouque D, Memboeuf A. Ion trap MS using high trapping gas pressure enables unequivocal structural analysis of three isobaric compounds in a mixture by using energy-resolved mass spectrometry and the survival yield technique. J. Mass Spectrom. JMS. 2020;55(7):e4478. https://doi.org/10.1002/jms.4478.
Article CAS PubMed Google Scholar
Jeanne Dit Fouque D, Maroto A, Memboeuf A. Structural analysis of a compound despite the presence of an isobaric interference by using in-source collision induced dissociation and tandem mass spectrometry. J. Mass Spectrom. JMS. 2021;56(2):e4698. https://doi.org/10.1002/jms.4698.
Article CAS PubMed Google Scholar
Crotti S, Menicatti M, Pallecchi M, Bartolucci G. Tandem mass spectrometry approaches for recognition of isomeric compounds mixtures. Mass Spectrom. Rev. n/a(n/a):e21757. https://doi.org/10.1002/mas.21757.
Menicatti M, Guandalini L, Dei S, Floriddia E, Teodori E, Traldi P, Bartolucci G. The power of energy-resolved tandem mass spectrometry experiments for resolution of isomers: the case of drug plasma stability investigation of multidrug resistance inhibitors. Rapid Commun. Mass Spectrom. RCM. 2016;30(3):423–32. https://doi.org/10.1002/rcm.7453.
Article CAS PubMed Google Scholar
Menicatti M, Guandalini L, Dei S, Floriddia E, Teodori E, Traldi P, Bartolucci G. Energy resolved tandem mass spectrometry experiments for resolution of isobaric compounds: a case of cis/trans isomerism. Eur. J. Mass Spectrom. Chichester Engl. 2016;22(5):235–43. https://doi.org/10.1255/ejms.1446.
Menicatti M, Pallecchi M, Bua S, Vullo D, Di Cesare Mannelli L, Ghelardini C, Carta F, Supuran CT, Bartolucci G. Resolution of co-eluting isomers of anti-inflammatory drugs conjugated to carbonic anhydrase inhibitors from plasma in liquid chromatography by energy-resolved tandem mass spectrometry. J. Enzyme Inhib. Med. Chem. 2018;33(1):671–9. https://doi.org/10.1080/14756366.2018.1445737.
Article CAS PubMed PubMed Central Google Scholar
Shang D, Kim M, Haberl M. Rapid and sensitive method for the determination of polycyclic aromatic hydrocarbons in soils using pseudo multiple reaction monitoring gas chromatography/tandem mass spectrometry. J. Chromatogr. A. 2014;1334:118–25. https://doi.org/10.1016/j.chroma.2014.01.074.
Article CAS PubMed Google Scholar
Galmiche M, Rodrigues A, Motsch E, Delhomme O, François Y-N, Millet M. The use of pseudo-MRM for a sensitive and selective detection and quantification of polycyclic aromatic compounds by tandem mass spectrometry. Rapid Commun. Mass Spectrom. 2022;36(13):e9307. https://doi.org/10.1002/rcm.9307.
Article CAS PubMed Google Scholar
Zhang H, Jia H, Gao Z, Xiang Y, Jiang T, Xu W. Parallel pseudo-MRM on the “brick” miniature mass spectrometer for high throughput multi-target screening. Talanta. 2023;252:123866. https://doi.org/10.1016/j.talanta.2022.123866.
Article CAS PubMed Google Scholar
Maroto, A.; Jeanne Dit Fouque, D.; Lartia, R.; Memboeuf, A. Removal of isobaric interferences in isotopic dilution mass spectrometry for the accurate quantification of a tryptic peptide by parallel pseudo-MRM and the survival yield technique. (in preparation).
Gabelica V, De Pauw E. Internal energy and fragmentation of ions produced in electrospray sources. Mass Spectrom. Rev. 2005;24(4):566–87. https://doi.org/10.1002/mas.20027.
Article CAS PubMed Google Scholar
Yan Z, Caldwell GW, Jones WJ, Masucci JA. Cone voltage induced in-source dissociation of glucuronides in electrospray and implications in biological analyses. Rapid Commun. Mass Spectrom. 2003;17(13):1433–42. https://doi.org/10.1002/rcm.1071.
Article CAS PubMed Google Scholar
Ramanathan R, Su A-D, Alvarez N, Blumenkrantz N, Chowdhury SK, Alton K, Patrick J. Liquid chromatography/mass spectrometry methods for distinguishing N-oxides from hydroxylated compounds. Anal. Chem. 2000;72(6):1352–9. https://doi.org/10.1021/ac9911692.
Article CAS PubMed Google Scholar
Huddleston MJ, Bean MF, Carr SA. Collisional fragmentation of glycopeptides by electrospray ionization LC/MS and LC/MS/MS: methods for selective detection of glycopeptides in protein digests. Anal. Chem. 1993;65(7):877–84. https://doi.org/10.1021/ac00055a009.
Article CAS PubMed Google Scholar
Chen H, Tabei K, Siegel MM. Biopolymer sequencing using a triple quadrupole mass spectrometer in the ESI nozzle-skimmer/precursor ion MS/MS mode. J. Am. Soc. Mass Spectrom. 2001;12(7):846–52. https://doi.org/10.1016/S1044-0305(01)00258-6.
Article CAS PubMed Google Scholar
Muth D, Marsden-Edwards E, Kachlicki P, Stobiecki M. Differentiation of isomeric malonylated flavonoid glyconjugates in plant extracts with UPLC-ESI/MS/MS. Phytochem. Anal. PCA. 2008;19(5):444–52. https://doi.org/10.1002/pca.1073.
Article CAS PubMed Google Scholar
Chen C-H, Lin Y-P, Lin J-L, Li S-T, Ren C-T, Wu C-Y, Chen C-H. Rapid identification of terminal sialic acid linkage isomers by pseudo-MS3 mass spectrometry. Isr. J. Chem. 2015;55(3–4):412–22. https://doi.org/10.1002/ijch.201400141.
Abdelhameed AS, Kadi AA, Attia MI, Angawi RF, Attwa MW, Darwish HW. Pseudo-MS3 approach using electrospray mass spectrometry (ESI-MS/MS) to characterize certain (2E)-2-[3-(1H-imidazol-1-Yl)-1-phenylpropylidene]hydrazinecarboxamide derivatives. J. Chem. 2014;2014:386301. https://doi.org/10.1155/2014/386301.
Abdelhameed AS, Attwa MW, Abdel-Aziz HA, Kadi AA. Induced in-source fragmentation pattern of certain novel (1Z,2E)-N-(Aryl)propanehydrazonoyl chlorides by electrospray mass spectrometry (ESI-MS/MS). Chem. Cent. J. 2013;7(1):16. https://doi.org/10.1186/1752-153X-7-16.
Article CAS PubMed PubMed Central Google Scholar
Carrier DJ, Eckers C, Wolff J-C. “In-source” fragmentation of an isobaric impurity of lamotrigine for its measurement by liquid chromatography tandem mass spectrometry after pre-concentration using solid phase extraction. J. Pharm. Biomed. Anal. 2008;47(4):731–7. https://doi.org/10.1016/j.jpba.2008.03.002.
Article CAS PubMed Google Scholar
Abrankó L, Szilvássy B. Mass spectrometric profiling of flavonoid glycoconjugates possessing isomeric aglycones. J. Mass Spectrom. JMS. 2015;50(1):71–80. https://doi.org/10.1002/jms.3474.
Article CAS PubMed Google Scholar
Hütteroth A, Putschew A, Jekel M. Selective detection of unknown organic bromine compounds and quantification potentiality by negative-ion electrospray ionization mass spectrometry with induced in-source fragmentation. Int. J. Environ. Anal. Chem. 2007;87(6):415–24. https://doi.org/10.1080/03067310601087684.
Massart DL, Vandeginste BGM, Buydens LMC, De Jong S, Lewi PJ, Smeyers-Verbeke J. Handbook of chemometrics and qualimetrics: Part A; Elsevier: Amsterdam. The Netherlands; 1997.
Kruve A, Rebane R, Kipper K, Oldekop M-L, Evard H, Herodes K, Ravio P, Leito I. Tutorial review on validation of liquid chromatography–mass spectrometry methods: Part I. Anal. Chim. Acta. 2015;870:29–44. https://doi.org/10.1016/j.aca.2015.02.017.
Article CAS PubMed Google Scholar
Maroto A, Boqué R, Riu J, Rius FX. Measurement uncertainty in analytical methods in which trueness is assessed from recovery assays. Anal. Chim. Acta. 2001;440(2):171–84. https://doi.org/10.1016/S0003-2670(01)01058-3.
International Organization for Standardization. ISO 5725-3, Accuracy (trueness and precision) of measurement methods and results. Geneva: ISO; 2023.
SLR Ellison, A Williams (Eds). Eurachem/CITAC guide: quantifying uncertainty in analytical measurement, third edition, (2012) ISBN 978-0-948926-30-3. Available from Www.Eurachem.Org.
Horwitz W, Albert R. The Horwitz Ratio (HorRat): a useful index of method performance with respect to precision. J. AOAC Int. 2006;89(4):1095–109. https://doi.org/10.1093/jaoac/89.4.1095.
Article CAS PubMed Google Scholar
Boyer KW, Horwitz W, Albert R. Interlaboratory variability in trace element analysis. Anal. Chem. 1985;57(2):454–9. https://doi.org/10.1021/ac50001a031.
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